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BSI PD CEN/TS 17083:2017

BSI PD CEN/TS 17083:2017

$142.49

Foodstuffs. Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)

Published By Publication Date Number of Pages
BSI 2017 26
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This Technical Specification specifies a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS). The method has been single-laboratory validated via the analysis of spiked samples (French fries (uncooked), bread, water biscuit, infant cereal, biscuit, green coffee, roast coffee and instant coffee), ranging from 30 ?g/kg to 1 500 ?g/kg acrylamide. The results from the single laboratory validation were obtained by a laboratory with significant experience in acrylamide analysis. In addition, this method has also been studied by inter laboratory trial via the analysis of samples containing incurred acrylamide, ranging from approximately 200 ?g/kg to 2 000 ?g/kg. Critical points of the method are identified in 7.5 and Clause 8.

PDF Catalog

PDF Pages PDF Title
2 undefined
6 1 Scope
2 Normative references
3 Principle
4 Reagents
8 5 Standard solution preparation
9 6 Apparatus
10 7 Procedure
7.1 General
11 7.2 Sample treatment
7.3 Test sample preparation
7.4 Bromination
7.5 Partition cleanup
12 8 GC-MS analysis
8.1 General
8.2 Injection conditions for split/splitless injector
8.3 Oven conditions
8.4 Column conditions
8.5 Transfer line conditions
8.6 Mass spectrometer conditions
13 8.7 Mass spectrometer acquisition parameters and peak identification
8.8 Calibration line
8.9 Sample analysis
14 9 Calculating and reporting
9.1 Calculation
9.2 Reporting
10 Test report
15 11 Precision data
11.1 Single laboratory validation
11.2 Interlaboratory trial
16 Annex A (informative)Typical chromatograms
18 Annex B (informative)GC-MS troubleshooting
B.1 General
19 B.2 Alternative GC columns
20 Annex C (informative)Single laboratory validation
22 Annex D (informative)Interlaboratory trial precision data

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BSI PD CEN/TS 17083:2017
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