ASTM-C169:2000 Edition
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C169-92(2000) Standard Test Methods for Chemical Analysis of Soda-Lime and Borosilicate Glass
Published By | Publication Date | Number of Pages |
ASTM | 2000 | 23 |
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1.1 These test methods cover the quantitative chemical analysis of soda-lime and borosilicate glass compositions for both referee and routine analysis. This would be for the usual constituents present in glasses of the following types: ( 1 ) soda-lime silicate glass, ( 2 ) soda-lime fluoride opal glass, and ( 3 ) borosilicate glass. The following common oxides, when present in concentrations greater than indicated, are known to interfere with some of the determinations in this method: 2 % barium oxide (BaO), 0.2 % phosphorous pentoxide (P 2 O 5 ), 0.05 % zinc oxide (ZnO), 0.05 % antimony oxide (Sb 2 O 3 ), 0.05 % lead oxide (PbO).
1.2 The analytical procedures, divided into two general groups, those for referee analysis, and those for routine analysis, appear in the following order:
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Fe 2 O 3 , TiO 2 , ZrO 2 by Photometry and Al 2 O 3 by Complexio-metric Titration | 16-22 |
---|---|
BaO, R 2O 2 (Al 2 O 3 + P 2 O 5 ), CaO, and MgO | 11-15 |
Colorimetric Determination of Ferrous Iron Using 1,10 Phenanthroline | 71-76 |
Fluorine by Pyrohydrolysis Separation and Specific Ion Electrode Measurement | 63-66 |
Procedures for Referee Analysis: | |
Al 2 O 3 , CaO, and MgO by Complexiometric Titration, and BaO, Na 2 O, and K 2 O by Gravimetric Method | 45-51 |
SO 3 (Total Sulfur) | 60 |
Na 2 O by the Zinc Uranyl Acetate Method and K 2 O by the Tetraphenylborate Method | 30-33 |
P 2 O 5 by the Molybdo-Vanadate Method | 67-70 |
Cr 2 O 3 by Volumetric and Photometric Methods | 23-25 |
B 2 O 3 | 61 to 62 |
MnO by the Periodate Oxidation Method | 26-29 |
Silica | 10 |
BaO, Al 2 O 3 , CaO, and MgO by Atomic Absorption; and Na 2 O and K 2 O by Flame Emission Spectroscopy | 52-59 |
Procedures for Routine Analysis: | |
Silica by the Single Dehydration Method | 42-44 |
As 2 O 3 by Volumetric Method | 36-40 |
Sections |
|
ICS Codes | 81.040.10 - Raw materials and raw glass |
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