ASTM-D5369 2008

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D5369-93(2008)e1 Standard Practice for Extraction of Solid Waste Samples for Chemical Analysis Using Soxhlet Extraction

Published By	Publication Date	Number of Pages
ASTM	2008	7

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Description

ASTM D5369-93-e1-Reapproved2008

Withdrawn Standard: Standard Practice for Extraction of Solid Waste Samples for Chemical Analysis Using Soxhlet Extraction (Withdrawn 2016)

ASTM D5369

Scope

1.1 This practice describes standard procedures for extracting nonvolatile and semivolatile organic compounds from solids such as soils, sediments, sludges, and granular wastes using Soxhlet extraction.

1.1.1 The sample must be suitable for being mixed with the sample drying agent, sodium sulfate or magnesium sulfate, to provide drying of all sample surfaces.

1.2 This practice, when used in conjunction with Test Method D 5368 is applicable to the determination of the total solvent extractable content (TSEC) of a soil, sediment, sludge, or granular solid waste and depends upon the solvent chosen for extraction.

1.3 This practice is limited to solvents having boiling points below the boiling point of water at ambient pressure.

1.4 The solvent extract obtained by this practice may be analyzed for total or specific nonvolatile and semivolatile organic compounds but may require sample clean-up procedures prior to specific compound analysis.

1.4.1 This practice provides sample extracts suitable for analysis by various techniques such as gas chromatography with flame ionization detection (GC/FID) or gas chromatography with mass spectrometric detection (GC/MS).

1.5 This practice is recommended only for solid samples that can pass through a 10-mesh sieve (approximately 2-mm openings), or are less than 2 mm in thickness.

1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautions see Section 9.

Keywords

nonvolatile; semivolatile; solid; samples; Extraction methods; Granular waste; Nonvolatile matter content–waste materials; Sediment; Semi-volatile organic/inorganic compounds; Sludge; Sludge sampling; Soil; Solvents–waste applications; Soxhlet extraction; TSEC (total solvent extractables content); Waste materials/processing/analysis

ICS Code

ICS Number Code n/a

DOI: 10.1520/D5369-93R08E01

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents
2	Terminology Summary of Practice Significance and Use Interferences TABLE 1
3	Selection of the Extraction Solvent Apparatus
4	Reagents and Materials Precautions Sample and Sample Preparation
5	Procedure
6	REFERENCES

Additional information

Standard Title	D5369-93(2008)e1 Standard Practice for Extraction of Solid Waste Samples for Chemical Analysis Using Soxhlet Extraction
Published Code	ASTM
Publication Date	2008
Pages Count	7