ASTM-D5384 2011

$35.75

D5384-11 Standard Test Methods for Chlorine in Used Petroleum Products (Field Test Kit Method)

Published By	Publication Date	Number of Pages
ASTM	2011	4

Guaranteed Safe Checkout

Category: ASTM

If you have any questions, feel free to reach out to our online customer service team by clicking on the bottom right corner. We’re here to assist you 24/7.
Email:[email protected]

Description

1.1 These test methods cover the determination of chlorine in used oils, fuels, and related materials, including: crankcase, hydraulic, diesel, lubricating and fuel oils, and kerosene, all containing <25 % (mass/mass) water.

1.1.1 Bromide and iodide are also titrated and reported on a molar basis as chlorine.

1.2 The entire analytical sequence, including sampling, sample pretreatment, chemical reactions, extraction, and quantification, is available in kit form using predispensed and encapsulated reagents. The overall objective is to provide a simple, easy to use procedure, permitting nontechnical personnel to perform a test in or outside of the laboratory environment in under 10 min. The test method also gives information to run the test without a kit.

1.2.1 Test Method A is preset to provide a greater than or less than result at 1000 mg/kg (ppm) total chlorine to meet regulatory requirements for used oils.

1.2.2 Test Method B provides results over a range from 200 to 4000 mg/kg total chlorine.

1.3 For both test methods, positive bias will result from samples that contain greater than 3 % (mass/mass) total sulfur. While a false negative result will not occur, other analytical methods should be used on high sulfur oils.

1.4 Test Method B, Lower Limit of Quantitation In the round-robin study to develop statistics for this test method, participants were asked to report results to the nearest 100 mg/kg. The lower limit of quantification could therefore only be determined to be in the range from 870 to 1180 mg/kg ⁵ .

1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety statements are given in Sections 3, 6, and 7.

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents Summary of Test Methods
2	Significance and Use Apparatus Reagents Sampling Procedure (Test Methods A and B)
3	Interpretation of Results Quality Control Precision and Bias TABLE 1
4	Keywords

Additional information

Standard Title	D5384-11 Standard Test Methods for Chlorine in Used Petroleum Products (Field Test Kit Method)
Published Code	ASTM
Publication Date	2011
Pages Count	4

Preview PDF


PDF Format	Searchable	Printable	Preview Now

ASTM-D5384 2011

PDF Catalog

Related products