ASTM-D86 2009

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D86-09e1 Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure

Published By	Publication Date	Number of Pages
ASTM	2009	27

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Category: ASTM

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Description

1.1 This test method covers the atmospheric distillation of petroleum products using a laboratory batch distillation unit to determine quantitatively the boiling range characteristics of such products as light and middle distillates, automotive spark-ignition engine fuels, automotive spark-ignition engine fuels containing up to 10 % ethanol, aviation gasolines, aviation turbine fuels, 1-D and 2-D diesel fuels, biodiesel blends up to 20 %, marine fuels, special petroleum spirits, naphthas, white spirits, kerosines, and Grades 1 and 2 burner fuels.

1.2 The test method is designed for the analysis of distillate fuels; it is not applicable to products containing appreciable quantities of residual material.

1.3 This test method covers both manual and automated instruments.

1.4 Unless otherwise noted, the values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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PDF Pages	PDF Title
1	Scope Referenced Documents
2	Terminology TABLE 1
3	Summary of Test Method Significance and Use Apparatus FIG. 1
4	FIG. 2
5	FIG. 3 FIG. 4 FIG. 5
6	Sampling, Storage, and Sample Conditioning Preparation of Apparatus TABLE 2
7	Calibration and Standardization TABLE 3
8	Procedure TABLE 4
9	FIG. 6
10	TABLE 5
11	Calculations TABLE 6
12	Report
13	Precision and Bias Keywords
14	A1. PRECISION TABLES FOR REPEATABILITY (r) AND REPRODUCIBILITY (R) A1.1 Tables
15	A2. DETAILED DESCRIPTION OF APPARATUS A2.1 Distillation Flasks A2.2 Condenser and Condenser Bath A2.3 Metal Shield or Enclosure for Flask A2.4 Heat Source A2.5 Flask Support
16	A2.6 Flask Support Board A2.7 A2.8 A2.9 Receiving Cylinders A2.10 Residue Cylinder FIG. A2.1
17	FIG. A2.2
18	FIG. A2.3 FIG. A2.4
19	A3. DETERMINATION OF THE DIFFERENCE IN LAG TIME BETWEEN AN ELECTRONIC TEMPERATURE MEASUREMENT SYSTEM AND A MERCURY-IN-GLASS THERMOMETER A3.1 A3.2 A3.3 A3.4 A3.5 A3.6 A4. PROCEDURE TO DETERMINE THE PERCENT EVAPORATED OR PERCENT RECOVERED AT A PRESCRIBED TEMPERATURE READING A4.1 A4.2 A4.3 A4.4 A4.5 Manual Distillation A4.6 Automated Distillation
20	A4.7 Calculations A4.8 Precision A4.9 A4.10 TABLE A4.1
21	TABLE A4.2 TABLE A4.3 TABLE A4.4 TABLE A4.5
22	X1. EXAMPLES ILLUSTRATING CALCULATIONS FOR REPORTING OF DATA X1.1 X1.2 Temperature Readings at Prescribed Percent Evaporated X2. EXAMPLES OF CALCULATION OF REPEATABILITY AND REPRODUCIBILITY OF VOLUME % (RECOVERED OR EVAPORATED) AT A PRESCRIBED TEMPERATURE READING X2.1 X2.2 Example Calculation FIG. X1.1
23	X3. TABLES OF CORRECTED LOSS FROM MEASURED LOSS AND BAROMETRIC PRESSURE X3.1 X3.2 TABLE X2.1 FIG. X3.1
24	X4. PROCEDURE TO EMULATE THE EMERGENT STEM ERROR OF A MERCURY-IN-GLASS THERMOMETER X4.1 X4.2 X4.3 X5. EXPLANATORY REPORT FORMS X5.1 FIG. X3.2
25	FIG. X5.1
26	FIG. X5.2

Additional information

Standard Title	D86-09e1 Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure
Published Code	ASTM
Publication Date	2009
Pages Count	27

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ASTM-D86 2009

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