ASTM-E2866 2012

$44.96

E2866-12 Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid

Published By	Publication Date	Number of Pages
ASTM	2012	15

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Categories: 13.080.10 - Chemical characteristics of soils, ASTM

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Description

ASTM E2866-12

Historical Standard: Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid

ASTM E2866

Scope

1.1 This procedure covers the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA) and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil. This method is based upon solvent extraction of a soil by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography/tandem mass spectrometry (LC/MS/MS). OPs are qualitatively and quantitatively determined by this method.

1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 The Method Detection Limit (MDL), electrospray ionization (ESI) mode and Reporting Range for the OPs are listed in Table 1.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

TABLE 1 Method Detection Limit and Reporting Range

Keywords

liquid chromatography; mass spectrometry; organophosphonates; pressurized fluid extraction; soil

ICS Code

ICS Number Code 13.080.10 (Chemical characteristics of soil)

DOI: 10.1520/E2866-12

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents TABLE 1
2	Terminology Summary of Test Method Significance and Use Interferences
3	Apparatus Reagents and Materials
4	Hazards Glassware Washing, Sampling and Preservation Preparation of LC/MS/MS Calibration and Standardization TABLE 2
5	TABLE 3
6	TABLE 4
7	TABLE 5
8	Pressurized Fluid Extraction Procedure TABLE 6
9	Calculation or Interpretation of Results Report Precision and Bias Keywords
10	TABLE 7 TABLE 8 TABLE 9
11	TABLE 10 TABLE 11 TABLE 12
12	TABLE 13 TABLE 14 TABLE 15
13	TABLE 16 TABLE 17 TABLE 18 TABLE 19
14	X1. TABLE 20 TABLE 21 TABLE 22 TABLE X1.1
15	FIG. X1.1

Additional information

Pinacolyl methylphosphonic acid	Negative
Ethyl methylphosphonic acid	Positive
Isopropyl methylphosphonic acid	Positive
Diisopropyl methylphosphonate	Positive
Methylphosphonic acid	Positive
ICS Codes	13.080.10 - Chemical characteristics of soils