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ASTM-E3 2007

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E3-01(2007) Standard Guide for Preparation of Metallographic Specimens

Published By Publication Date Number of Pages
ASTM 2007 12
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1.1 The primary objective of metallographic examinations is to reveal the constituents and structure of metals and their alloys by means of a light optical or scanning electron microscope. In special cases, the objective of the examination may require the development of less detail than in other cases but, under nearly all conditions, the proper selection and preparation of the specimen is of major importance. Because of the diversity in available equipment and the wide variety of problems encountered, the following text presents for the guidance of the metallographer only those practices which experience has shown are generally satisfactory; it cannot and does not describe the variations in technique required to solve individual specimen preparation problems.

Note 1 – For a more extensive description of various metallographic techniques, refer to Samuels, L. E., Metallographic Polishing by Mechanical Methods , American Society for Metals (ASM) Metals Park, OH, 3rd Ed., 1982; Petzow, G., Metallographic Etching, ASM, 1978; and VanderVoort, G., Metallography: Principles and Practice , McGraw Hill, NY, 2nd Ed., 1999.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Significance and Use
2 Selection of Metallographic Specimens
Size of Metallographic Specimens
FIG. 1
3 Cutting of Metallographic Specimens
Cleanliness
Mounting of Specimens
TABLE 1
4 Plating of Specimens
TABLE 2
5 Grinding and Polishing
TABLE 3
TABLE 4
6 Special Procedures
TABLE 5
7 TABLE 6
TABLE 7
8 Precision and Bias
Keywords
X1. CLEANING SPECIMENS
X1.1
X1.2
X1.3
9 X2. APPLIED LOAD CONVERSIONS
X2.1
X2.2
X2.3
TABLE X1.1
10 X2.4
X3. PROCEDURE IMPROVEMENT
X3.1
X3.2
X3.3
X3.4
X3.5
X3.6
X3.7
X3.8
X3.9
X3.10
X3.11
11 X3.12
X3.13
X3.14
X3.15
X3.16
REFERENCES
ASTM-E3 2007
$44.96