ASTM-F2013:2010 Edition
$40.63
F2013-10 Standard Test Method for Determination of Residual Acetaldehyde in Polyethylene Terephthalate Bottle Polymer Using an Automated Static Head-Space Sampling Device and a Capillary GC with a Flame Ionization Detector
Published By | Publication Date | Number of Pages |
ASTM | 2010 | 11 |
ASTM F2013-10
Historical Standard: Standard Test Method for Determination of Residual Acetaldehyde in Polyethylene Terephthalate Bottle Polymer Using an Automated Static Head-Space Sampling Device and a Capillary GC with a Flame Ionization Detector
ASTM F2013
Scope
1.1 This test method covers a gas chromatographic procedure for the determination of the ppm residual acetaldehyde (AA) present in poly(ethylene terephthalate) (PET) homo-polymers and co-polymers which are used in the manufacture of beverage bottles. This includes sample types of both amorphous and solid-stated pellet and preform samples, as opposed to the bottle test, Test Method D4509, an acetaldehyde test requiring 24 h of desorption time at 23°C into the bottle headspace and then the concentration of the headspace quantified by a similar GC method.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Keywords
AA test; acetaldehyde; carbonated soft drink; ground parison AA; PET bottles; 24 hours headspace; water; Acetaldehyde (AA); Flame ionization detectors (FID); Headspace gas chromatography; Headspace sampler; Polyethylene terephthalate bottle polymer; Polymers
ICS Code
ICS Number Code 55.100 (Bottles. Pots. Jars)
DOI: 10.1520/F2013-10
PDF Catalog
PDF Pages | PDF Title |
---|---|
1 | Scope Referenced Documents Terminology Summary of Test Method Significance and Use Sources of Error |
2 | Apparatus Reagents and Materials Calibration and Standardization Sample Preparation |
3 | Procedure Calculation Report Precision and Bias |
4 | Keywords X1. HEWLETT-PACKARD 6890 SERIES GC CONDITIONS TABLE X1.1 |
5 | X2. HEWLETT-PACKARD 7694 HEAD-SPACE SAMPLER CONDITIONS TABLE X2.1 |
6 | X3. HEWLETT-PACKARD 6890 SERIES INTEGRATOR METHOD FILE FIG. X3.1 |
7 | FIG. X3.1 |
8 | FIG. X3.1 |
9 | X4. CHROMATOGRAM OF A TYPICAL SAMPLE FIG. X4.1 |
10 | X5. PREPARATION OF ACETALDEHYDE CALIBRATION STANDARDS X5.1 Introduction X5.2 Materials X5.3 Setup X5.4 Procedure X5.5 Labeling |