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BS EN ISO 2719:2002:2004 Edition

$167.15

Determination of flash point. Pensky-Martens closed cup method

Published By Publication Date Number of Pages
BSI 2004 34
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PDF Pages PDF Title
5 TitlePage – Determination of flash point�— Pensky- Martens closed cup method
7 TableofContent – Contents Page
8 Foreword – Foreword
9 Introduction – Introduction
11 Scope – 1��� Scope
NormativeReference – 2��� Normative references
12 Clause1 – 4��� Principle
Clause1 – 5��� Chemicals and materials
UntitledSubclause2 – 5.1��� Cleaning solvent
UntitledSubclause2 – 5.2��� Verification liquids
Clause1 – 6��� Apparatus
UntitledSubclause2 – 6.1��� Flash point apparatus
UntitledSubclause2 – 6.2��� Thermometers
UntitledSubclause2 – 6.3��� Barometer
13 UntitledSubclause2 – 6.4��� Heating bath or oven
Clause1 – 7��� Apparatus preparation
Subclause2 – 7.1��� Location of the apparatus
Subclause2 – 7.2��� Cleaning the test cup
Subclause2 – 7.3��� Apparatus assembly
Subclause2 – 7.4��� Apparatus verification
UntitledSubclause3 – 7.4.1��� Verify the correct functioning of the apparatus at least once a yea…
UntitledSubclause3 – 7.4.2��� The numerical values obtained during the verification check shall n…
Clause1 – 8��� Sampling
UntitledSubclause2 – 8.1��� Unless otherwise specified, obtain samples for analysis in accordance…
UntitledSubclause2 – 8.2��� Place samples in tightly sealed containers, appropriate to the materi…
UntitledSubclause2 – 8.3��� Store the samples in conditions that minimize vapour loss and pressur…
14 Clause1 – 9��� Sample handling
Subclause2 – 9.1��� Petroleum products
Subclause3 – 9.1.1��� Subsampling
Subclause3 – 9.1.2��� Samples containing undissolved water
Subclause3 – 9.1.3��� Samples that are liquid at ambient temperature
Subclause3 – 9.1.4��� Samples that are semi-solid or solid at ambient temperature
Subclause2 – 9.2��� Paints and varnishes
Clause1 – 10��� Procedure
Subclause2 – 10.1��� General
Subclause2 – 10.2��� Procedure�A
UntitledSubclause3 – 10.2.1��� Using a barometer (
UntitledSubclause3 – 10.2.2��� Fill the test cup (see�
15 UntitledSubclause3 – 10.2.3��� When the test portion is expected to have a flash point of
UntitledSubclause3 – 10.2.4��� When the test portion is expected to have a flash point of above
UntitledSubclause3 – 10.2.5��� When testing a material of unknown flash point, conduct a prelimin…
UntitledSubclause3 – 10.2.6��� Record, as the observed flash point, the temperature of the test p…
UntitledSubclause3 – 10.2.7��� When the temperature at which the flash point is observed is less …
Subclause2 – 10.3��� Procedure�B
UntitledSubclause3 – 10.3.1��� Using a barometer (
UntitledSubclause3 – 10.3.2��� Fill the test cup (see�
UntitledSubclause3 – 10.3.3��� With the exception of the requirements given in
Clause1 – 11��� Calculation
Subclause2 – 11.1��� Conversion of barometric pressure reading
16 Subclause2 – 11.2��� Correction of observed flash point to standard atmospheric pressure
Clause1 – 12��� Expression of results
Clause1 – 13��� Precision
Subclause2 – 13.1��� General
Subclause2 – 13.2��� Repeatability,
17 Subclause2 – 13.3��� Reproducibility,
Clause1 – 14��� Test report
18 AnnexInformative – Apparatus verification
Clause1 – A.1��� General
Clause1 – A.2��� Verification check standards
UntitledSubclause2 – A.2.1��� Certified reference material (CRM)
UntitledSubclause2 – A.2.2��� Secondary working standard (SWS)
Clause1 – A.3��� Procedure
UntitledSubclause2 – A.3.1��� Chose a CRM or SWS which falls within the range of flash points to …
19 UntitledSubclause2 – A.3.2��� For new apparatus, and at least once a year for working apparatus, …
UntitledSubclause2 – A.3.3��� For intermediate verification, conduct a verification check using a…
UntitledSubclause2 – A.3.4��� Correct the result for barometric pressure in accordance with
Clause1 – A.4��� Evaluation of test result
UntitledSubclause2 – A.4.1��� General
UntitledSubclause3 – A.4.1.1��� Single test
UntitledSubclause3 – A.4.1.2��� Multiple tests
20 UntitledSubclause2 – A.4.2��� If the test result conforms to the tolerance requirements, record t…
UntitledSubclause2 – A.4.3��� If the result does not conform to the tolerance requirements and a …
UntitledSubclause2 – A.4.4��� If the test result still does not conform to the tolerance requirem…
21 AnnexNormative – Pensky-Martens closed cup test apparatus
Clause1 – B.1��� General
Clause1 – B.2��� Test cup
Clause1 – B.3��� Cover assembly
UntitledSubclause2 – B.3.1��� The cover assembly shall comprise the following items.
UntitledSubclause2 – B.3.2��� Lid
UntitledSubclause2 – B.3.3��� Shutter
UntitledSubclause2 – B.3.4��� Flame-exposure device
UntitledSubclause2 – B.3.5��� Pilot flame for automatic relighting of the exposure-flame
22 UntitledSubclause2 – B.3.6��� Stirring device
Clause1 – B.4��� Heating chamber and top plate
27 AnnexNormative – Thermometer specifications
28 AnnexInformative – Adaptor for low-range thermometer
Clause1 – D.1��� General
Clause1 – D.2��� Test gauge
31 Bibliography – Bibliography
BS EN ISO 2719:2002
$167.15