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BS ISO 10258:2018

$142.49

Copper sulfide concentrates. Determination of copper content. Titrimetric methods

Published By Publication Date Number of Pages
BSI 2018 28
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This document specifies two titrimetric methods for the determination of the copper content of copper sulfide concentrates in the range 15 % (m/m) to 50 % (m/m), using sodium thiosulfate after separation (method 1) or without separation (method 2) of copper from interfering elements.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
4.1 Method 1 (Long iodide method)
4.2 Method 2 (Short iodide method)
8 5 Reagents
10 6 Apparatus
7 Sample
7.1 Test sample
7.2 Test portion
8 Procedure
8.1 Number of determinations
11 8.2 Blank test
8.3 Determination — Method 1: Long iodide method
8.3.1 Decomposition of test portion
8.3.2 Separation of copper
12 8.3.3 Dissolution of copper precipitate
8.3.4 Titration
8.3.5 FAAS determination of copper in the insoluble residue, filtrate, and filter paper
13 8.4 Determination — Method 2: Short iodide method
8.4.1 Decomposition of the test portion
8.4.2 Titration
14 9 Expression of results
10 Precision
10.1 Expression of precision
15 10.2 Method for obtaining the final result (see Annex B)
10.3 Precision between laboratories
16 10.4 Check of trueness
17 11 Test report
18 Annex A (informative) Procedure for the preparation and determination of the mass of a predried test portion
20 Annex B (normative) Flowsheet of the procedure for the acceptance of analytical values for test samples
21 Annex C (informative) Derivation of precision formulae
26 Bibliography
BS ISO 10258:2018
$142.49