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BSI PD ISO/TR 18818:2017

$102.76

Cosmetics. Analytical method. Detection and quantitative determination of Diethanolamine (DEA) by GC/MS

Published By Publication Date Number of Pages
BSI 2017 16
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This document describes a screening method for rapid sampling and identifying of diethanolamine (DEA) in cosmetics and raw materials used in cosmetics by gas chromatography – mass spectroscopy (GC-MS).

This method is not applicable to the detection and/or quantification of DEA-related ingredients. When this method is used to analyse unfamiliar sample matrices analysts are advised to confirm the applicability and flexibility of the techniques in their matrix.

Under the conditions specified this method is reliable for quantification with DEA level at 1 000 mg/kg (0,1 %).

However, samples with lower concentrations (<0,1 %) or otherwise unusual compositions or characteristics can present difficulties (such as, for example, peak tailing) that preclude the direct use of this method.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
8 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
9 5 Procedure
5.1 Preparation of calibration solutions
5.1.1 Stock solution
5.1.2 Standard solution
5.1.3 Calibration solutions
5.2 Sample preparation
5.3 Analysis
5.3.1 General
10 5.3.2 Example of instrumental conditions
5.3.3 Recovery
5.3.4 Calibration curve
11 5.4 Determination
6 Limit of quantification
12 Annex A (informative) Examples of typical GC-MS chromatogram of standard DEA
14 Bibliography
BSI PD ISO/TR 18818:2017
$102.76