ISO 3329:1975
$12.35
Ammonium nitrate for industrial use — Determination of content of sulphur compounds — Method by reduction and titrimetry
Published By | Publication Date | Number of Pages |
ISO | 1975-07 | 6 |
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Applicable to products the content of which, expressed as sulphate, is equal to or more than 0.0005 % (m/m). Heating of a test portion in the presence of sodium carbonate, in a fume-cupboard, until the ammonium salts have been eliminated (about 300 °C). Reduction of the sulphureous residue to sulphides by a mixture of hydriodic acid and hypophosphorus acid. Absorption of the hydrogen sulphide evolved in a mixture of sodium hydroxide solution and acetone. Titration of the sulphide with standard volumetric mercury(II) acetate solution in the presence of dithizone as indicator. A typical apparatus for reduction and distillation is shown in a figure.
Published Code | ISO |
---|---|
Published By | International Organization for Standardization |
Publication Date | 1975-07 |
Pages Count | 6 |
Language | English |
Edition | 1 |
File Size | 317.4 KB |
ICS Codes | 71.060.50 - Salts |
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