{"id":291093,"date":"2024-10-19T19:45:41","date_gmt":"2024-10-19T19:45:41","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-196192018\/"},"modified":"2024-10-25T16:47:05","modified_gmt":"2024-10-25T16:47:05","slug":"bs-iso-196192018","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-196192018\/","title":{"rendered":"BS ISO 19619:2018"},"content":{"rendered":"
This document specifies an analytical procedure for the determination of free propylene oxide in surfactants which are synthesized from propylene oxide copolymers.<\/p>\n
The method is appropriate for the qualitative and quantitative determination of propylene oxide groups in propylene oxide adducts, polyethers and polyglycol esters by headspace gas chromatography (HS-GC) with a flame ionization detector (FID) based on external procedure. Gas chromatography-mass spectrometry (GC-MS) is used for the confirmatory purposes.<\/p>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
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2<\/td>\n | National foreword <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | Foreword <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Principles 5 Reagents <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 6 Apparatus <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 7 Preparation of calibration solutions 7.1 Standard solutions 7.1.1 General 7.1.2 Difference weighing 7.1.3 Commercial standard vial 7.2 Calibration solutions <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 8 Sampling and preparation of the test sample 8.1 Preparation of the test sample 8.2 Determination 8.3 Qualitative determination 8.4 Quantitative determination <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 9 Chromatographic and mass spectrometer conditions <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 10 Evaluation 10.1 General 10.2 Identification <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 10.3 Calculation <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 11 Precision 11.1 Repeatability 11.2 Reproducibility limit 12 Test report <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | Annex A (informative) Statistical data from the ring carried out <\/td>\n<\/tr>\n | ||||||
18<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Surface active agents. Determination of free propylene oxide content in propylene oxide adduct surfactants. GC method<\/b><\/p>\n |