{"id":66471,"date":"2024-10-17T13:03:59","date_gmt":"2024-10-17T13:03:59","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-d5863-2011\/"},"modified":"2024-10-24T18:30:08","modified_gmt":"2024-10-24T18:30:08","slug":"astm-d5863-2011","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-d5863-2011\/","title":{"rendered":"ASTM-D5863 2011"},"content":{"rendered":"<\/p>\n<p id=\"s00002\">1.1 These test methods cover the determination of nickel, vanadium, iron, and sodium in crude oils and residual fuels by flame atomic absorption spectrometry (AAS). Two different test methods are presented.<\/p>\n<p id=\"s00003\">1.2 <span class=\"italic\"><span class=\"italic\">Test Method A, Sections<\/span> 7 13<\/span> Flame AAS is used to analyze a sample that is decomposed with acid for the determination of total Ni, V, and Fe.<\/p>\n<p id=\"s00004\">1.3 <span class=\"italic\"><span class=\"italic\">Test Method B, Sections<\/span> 14 19<\/span> Flame AAS is used to analyze a sample diluted with an organic solvent for the determination of Ni, V, and Na. This test method uses oil-soluble metals for calibration to determine dissolved metals and does not purport to quantitatively determine nor detect insoluble particulates. Hence, this test method may underestimate the metal content, especially sodium, present as inorganic sodium salts.<\/p>\n<p id=\"s00005\">1.4 The concentration ranges covered by these test methods are determined by the sensitivity of the instruments, the amount of sample taken for analysis, and the dilution volume. A specific statement is given in Note 1.<\/p>\n<p id=\"s00006\">1.5 For each element, each test method has its own unique precision. The user can select the appropriate test method based on the precision required for the specific analysis.<\/p>\n<p id=\"s00007\">1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.<\/p>\n<p id=\"s00008\">1.7 <span class=\"italic\">This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. <span class=\"med\">Specific warning statements are given in 7.1, 8.2, 8.5, 10.2, 10.4, and 15.1.<\/span><\/span><\/p>\n<p><h4>PDF Catalog<\/h4>\n<table border=\"1px\" class=\"des-table\">\n<tr>\n<th>PDF Pages<\/th>\n<th>PDF Title<\/th>\n<\/tr>\n<tr>\n<td><b>1<b><\/td>\n<td>Scope <br \/> Referenced Documents <br \/> Summary of Test Method  <\/td>\n<\/tr>\n<tr>\n<td><b>2<b><\/td>\n<td>Significance and Use <br \/> Purity of Reagents <br \/> Sampling and Sample Handling <br \/> Apparatus <br \/> Reagents <br \/> FIG. 1   <\/td>\n<\/tr>\n<tr>\n<td><b>3<b><\/td>\n<td>Preparation of Standards <br \/> Preparation of Test Solutions <br \/> FIG. 2  <br \/> TABLE 1  <\/td>\n<\/tr>\n<tr>\n<td><b>4<b><\/td>\n<td>Preparation of Apparatus <br \/> Calibration and Analysis <br \/> Quality Assurance\/Quality Control (QA\/QC) <br \/> Apparatus <br \/> Reagents <br \/> Preparation of Standards and Test Solutions <br \/> TABLE 2  <\/td>\n<\/tr>\n<tr>\n<td><b>5<b><\/td>\n<td>Preparation of Apparatus <br \/> Calibration and Analysis <br \/> Quality Assurance\/Quality Control (QA\/QC) <br \/> Calculation <br \/> Report <br \/> Precision and Bias <br \/> Keywords <br \/> TABLE 3  <\/td>\n<\/tr>\n<tr>\n<td><b>6<b><\/td>\n<td>X1. GENERIC QUALITY CONTROL STATEMENT FOR D02 TEST METHODS <br \/> X1.1  <br \/> X1.2  <br \/> X1.3  <br \/> X1.4  <br \/> X1.5  <br \/> TABLE 4 <br \/> TABLE 5 <br \/> TABLE 6  <\/td>\n<\/tr>\n<tr>\n<td><b>7<b><\/td>\n<td>X1.6  <br \/> X2. AIDS TO THE ANALYST <br \/> X2.1  <br \/> X2.2  <br \/> X2.3  <br \/> X2.4  <br \/> X2.5  <br \/> X2.6  <br \/> X2.7  <br \/> X2.8  <br \/> X2.9  <br \/> X2.10  <br \/> X2.11  <br \/> X2.12  <br \/> X2.13  <br \/> X2.14  <br \/> X2.15  <br \/> X2.16  <br \/> X2.17   <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"<p><b>D5863-00a(2011) Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry<\/b><\/p>\n<table class=\"shortdes-table\" style=\"width: 100%\" border=\"0\" cellspacing=\"0\" cellpadding=\"0\">\n<tbody>\n<tr>\n<td>Published By<\/td>\n<td>Publication Date<\/td>\n<td>Number of Pages<\/td>\n<\/tr>\n<tr>\n<td><a href=\"https:\/\/pdfstandards.shop\/product-category\/publishers\/astm\/\"><b>ASTM<\/b><\/a><\/td>\n<td>2011<\/td>\n<td>7<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":66472,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2637],"product_tag":[],"class_list":{"0":"post-66471","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-astm","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/66471","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/66472"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=66471"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=66471"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=66471"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}