ASTM-C997 1993
$63.38
C997-83(1993)e1 Test Methods for Chemical and Instrumental Analysis of Nuclear-Grade Sodium and Cover Gas (Withdrawn 1999)
| Published By | Publication Date | Number of Pages |
| ASTM | 1993 | 53 |
ASTM C997-83-e1-Reapproved1993
Withdrawn Standard: Test Methods for Chemical and Instrumental Analysis of Nuclear-Grade Sodium and Cover Gas (Withdrawn 1999)
ASTM C997
Scope
1.1 These test methods provide instructions for performing chemical, radiochemical, and instrumental analyses of sodium metal and for determining impurities in cover gas.
1.2 The analytical procedures appear in the following order:
Sections Bypass Sampling 6 to 12 Overflow Sampling 13 to 18 Wire and Foil Equilibration Sampling 19 to 24 Laboratory Distillation of Sodium 25 to 31 Hydrogen by Hydrogen-Diffusion Meter 32 to 37 Carbon by Oxyacidic-Flux Method 38 to 46 Carbonaceous Gases Released by Acid 47 to 54 Cyanide by Spectrophotometry 55 to 64 Oxygen by the Equilibration Method Using Vanadium Wires 65 to 74 Fluoride by Selective Ion Electrode 75 to 83 Chloride by Selective Ion Electrode 84 to 92 Trace Metals by Atomic Absorption or Flame Emission 93 to 101 Spectrophotometry Cadmium and Zinc by Atomic Absorption Spectrophotometry 102 to 111 Potassium by Atomic Absorption Spectrophotometry 112 to 121 Rubidium and Cesium by Flame Spectrometry 122 to 131 Silicon by Spectrophotometry 132 to 140 Boron by Spectrophotometry 141 to 149 Uranium by Fluorimetry 150 to 157 Oxygen by Oxygen Meter 158 to 164 Carbon by Equilibration Method 165 to 172 Hydrogen by Equilibration Method 173 to 180 Sulfur by Spectrophotometry 181 to 189 Sodium Purity By Titration 190 to 199 Plutonium by Alpha Assay 200 to 209 Gamma Assay of Distillation Residue 210 to 217 Gamma Assay of Sodium Solution 218 to 226 Radioactive Iodine by Gamma Counting 227 to 235 Tritium by Liquid Scintillation Counting 236 to 245 Particles by Filtration 246 to 254 Gaseous Impurities in Cover Gas by Gas Chromatography 255 to 263
Keywords
Boron content-nuclear-grade materials; Cadmium content; Carbon content-nuclear materials; Cesium content; Chloride content-nuclear applications; Cyanides content; Distillation; Fluoride content; Gamma radiation; Gas chromatography-nuclear; Gases-radioactive; Hydrogen content-nuclear materials; Impurities-nuclear materials; Iodine-radioactive; Nuclear fuels (reactor); Oxygen content; Plutonium-isotopic analysis; Potassium content; Rubidium content; Sampling-nuclear/related energy sources; Silicon content; Sodium-nuclear applications; Solids content; Sulfur content-nuclear materials; Trace elements content-nuclear materials; Tritium content; Uranium content; Zinc content; sodium/cover gas (nuclear-grade)- chemical/instrumental analysis,; methods
ICS Code
ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)
DOI:
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 1 | Scope Referenced Documents Significance and Use Reagents Safety Precautions |
| 2 | Scope Summary of Method Apparatus Reagents and Materials Precautions Procedure FIG. 1 |
| 3 | Discussion Scope Summary of Method Apparatus TABLE 1 FIG. 2 |
| 4 | Precautions Procedure FIG. 3 FIG. 4 |
| 5 | FIG. 5 |
| 6 | Discussion Scope Summary of Method Apparatus |
| 7 | Precautions Procedure Discussion Scope Summary of Method Apparatus Reagents and Materials FIG. 6 |
| 8 | Precautions Procedure FIG. 7 |
| 9 | Discussion FIG. 8 FIG. 9 |
| 10 | Scope Summary of Method Apparatus Procedure FIG. 10 FIG. 11 |
| 11 | Calculation Precision and Accuracy Scope Summary of Method Apparatus FIG. 12 |
| 12 | FIG. 13 FIG. 14 FIG. 15 |
| 13 | Reagents and Materials Preparation of Apparatus Calibration of Chromatograph FIG. 16 FIG. 17 |
| 14 | Procedure FIG. 18 |
| 15 | Calculation Precision and Accuracy Scope Summary of Method Apparatus |
| 16 | Reagents and Materials Calibration of Chromatograph Procedure FIG. 19 FIG. 20 |
| 17 | FIG. 21 FIG. 22 |
| 18 | Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus FIG. 23 |
| 19 | Reagents and Materials Precautions Calibration Procedure |
| 20 | Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus FIG. 24 |
| 21 | Reagents and Materials Precautions Calibration of Vacuum-Fusion Analyzer Procedure FIG. 25 FIG. 26 |
| 22 | TABLE 2 |
| 23 | Calculation Precision and Accuracy |
| 24 | Scope Summary of Method Interferences Apparatus Reagents and Materials Calibration Procedure TABLE 3 |
| 25 | Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials Calibration Procedure Calculation |
| 26 | Precision and Accuracy Scope Summary of Method Apparatus Reagents and Materials TABLE 4 |
| 27 | Precautions Calibration Procedure TABLE 5 |
| 28 | Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials Precautions TABLE 6 |
| 29 | Calibration Procedure Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials |
| 30 | Precautions Calibration Procedure Calculation Precision and Accuracy Scope |
| 31 | Summary of Method Interferences Apparatus Reagents and Materials Precautions Calibration Procedure |
| 32 | Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials Calibration |
| 33 | Procedure Calculation Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials |
| 34 | Calibration Procedure Calculation Precision and Accuracy Scope Summary of Method Apparatus Reagents and Materials |
| 35 | Calibration Procedure Calculation Precision and Accuracy Scope Summary of Method Apparatus Precautions |
| 36 | Calibration Procedure Precision and Accuracy Scope Summary of Method Apparatus Reagents and Materials FIG. 27 |
| 37 | Calibration Procedure Calculation Precision and Accuracy Scope Summary of Method Apparatus |
| 38 | Reagents and Materials Calibration Procedure Calculation Precision and Accuracy Scope Summary of Method Apparatus |
| 39 | Reagents and Materials Precautions Calibration Procedure Calculation FIG. 28 |
| 40 | Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials Precautions Calibration Procedure |
| 41 | Calculation |
| 42 | Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials |
| 43 | Precautions FIG. 29 FIG. 30 |
| 44 | Calibration Procedure FIG. 31 |
| 45 | Calculation Precision and Accuracy Scope Summary of Method Apparatus Reagents and Materials Calibration Procedure Calculation Precision and Accuracy Scope |
| 46 | Summary of Method Apparatus Reagents and Materials Precautions Calibration Procedure Calculation Precision and Accuracy Scope Summary of Method |
| 47 | Apparatus Reagents and Materials Precautions Calibration Procedure Calculation |
| 48 | Precision and Accuracy Scope Summary of Method Interferences Apparatus Reagents and Materials Precautions Calibration Procedure |
| 49 | Calculation Precision and Accuracy Scope Summary of Method Apparatus FIG. 32 |
| 50 | Reagents and Materials Precleaning and Testing Sampling Procedure Calculation Precision and Accuracy Scope |
| 51 | Summary of Method Apparatus TABLE 7 |
| 52 | Reagents and Materials Precautions Calibration Procedure FIG. 33 |
| 53 | Calculation Precision and Accuracy Keywords REFERENCES |
