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ASTM-D934 2003

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D934-80(2003) Standard Practices for Identification of Crystalline Compounds in Water-Formed Deposits By X-Ray Diffraction

Published By Publication Date Number of Pages
ASTM 2003 9
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1.1 These practices provide for X-ray diffraction analysis of powdered crystalline compounds in water-formed deposits. Two are given as follows:

1.2 Both practices yield qualitative identification of crystalline components of water-formed deposits for which X-ray diffraction data are available or can be obtained. Greater difficulty is encountered in identification when the number of crystalline components increases.

1.3 Amorphous phases cannot be identified without special treatment. Oils, greases, and most organic decomposition products are not identifiable.

1.4 The sensitivity for a given component varies with a combination of such factors as density, degree of crystallization, particle size, coincidence of strong lines of components and the kind and arrangement of the atoms of the components. Minimum percentages for identification may therefore range from 1 to 40 %.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8 and Note 20.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of Practices
Significance and Use
Purity of Reagents
2 Sampling
Safety Precautions
Preliminary Testing of Analytical Sample
Preparation of Sample
Selective Segregation of Analytical Sample
3 Scope
Summary of Practice A
Interferences
4 Apparatus
Reagents and Material
Preparation of Test Specimen
Calibration and Standardization
5 TABLE 1
6 Procedure for Taking Patterns
Identification of Patterns

7 Report
Scope
Summary of Practice
Interferences
Apparatus
X-Ray Equipment Preparation
Calibration and Standardization
8 Procedure
Identification of Patterns

Report
Keywords

9 REFERENCES
FIG. 1
ASTM-D934 2003
$40.63