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ASTM-E384 2011

$63.38

E384-11e1 Standard Test Method for Knoop and Vickers Hardness of Materials

Published By Publication Date Number of Pages
ASTM 2011 43
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ASTM E384-11e1

Historical Standard: Standard Test Method for Knoop and Vickers Hardness of Materials

ASTM E384

Scope

1.1 This test method covers determination of the Knoop and Vickers hardness of materials, the verification of Knoop and Vickers hardness testing machines, and the calibration of standardized Knoop and Vickers test blocks.

1.2 This test method covers Knoop and Vickers hardness tests made utilizing test forces in micro (9.807 × 10-3 to 9.807 N ) ( 1 to 1000 gf ) and macro (>9.807 to 1176.80 N) ( >1kg to 120 kgf ) ranges.

Note 1—Previous versions of this standard limited test forces to 9.807 N (1 kgf).

1.3 This test method includes all of the requirements to perform macro Vickers hardness tests as previously defined in Test Method E92, Standard Test Method for Vickers Hardness Testing.

1.4 This test method includes an analysis of the possible sources of errors that can occur during Knoop and Vickers testing and how these factors affect the accuracy, repeatability, and reproducibility of test results.

Note 2—While Committee E04 is primarily concerned with metals, the test procedures described are applicable to other materials.

1.5 UnitsWhen Knoop and Vickers hardness tests were developed, the force levels were specified in units of grams-force (gf) and kilograms-force (kgf). This standard specifies the units of force and length in the International System of Units (SI); that is, force in Newtons (N) and length in mm or μm. However, because of the historical precedent and continued common usage, force values in gf and kgf units are provided for information and much of the discussion in this standard as well as the method of reporting the test results refers to these units.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

hardness; indentation; Knoop; microindentation; macroindentation; Vickers; Abb´e-Nelson illumination; Calibration–metals/alloys analysis instrumentation; Hardness (indentation)–microhardness; Indenter geometry; Knoop hardness (HK) number; Kohler illumination; Metallic hardness; Metals and metallic materials; Repeatability/reproducibility (RR); Structural metals/alloys; Verification; Vickers hardness (HV)

ICS Code

ICS Number Code 19.060 (Mechanical testing)

DOI: 10.1520/E0384-11E01

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
2 Terminology
FIG. 1
3 Significance and Use
Principle of Test
FIG. 2
4 Apparatus
5 Test Specimen
6 Procedure
TABLE 1
TABLE 2
7 TABLE 3
8 Report
Precision and Bias
TABLE 4
9 FIG. 3
TABLE 5
10 TABLE 6
11 TABLE 7
12 TABLE 8
13 Conversion to Other Hardness Scales or Tensile Strength Values
Keywords
TABLE 9
14 TABLE 10
FIG. 4
15 FIG. 5
FIG. 6
16 FIG. 7
TABLE 11
TABLE 12
TABLE 13
17 A1. VERIFICATION OF KNOOP AND VICKERS HARDNESS TESTING MACHINES AND INDENTERS
A1.1 Scope
A1.2 General Requirements
A1.3 Direct Verification
TABLE 14
TABLE 15
TABLE A1.1
18 A1.4 Indirect Verification
TABLE A1.2
TABLE A1.3
19 FIG. A1.1
TABLE A1.4
20 A1.5 Weekly Verification
TABLE A1.5
TABLE A1.6
21 A1.6 Verification Report
A1.7 Example Calculations of Repeatability and Error
22 A2. REQUIREMENTS FOR STANDARDIZED HARDNESS TEST BLOCKS USED TO VERIFY KNOOP AND VICKERS HARDNESS TEST MACHINES
A2.1 Scope
A2.2 Accreditation
A2.3 Test Block Manufacture
A2.4 Standardizing Tester Requirements
A2.5 Test Block Standardization Procedure
A2.6 Repeatability of the Standardized Test Block
23 A2.7 Marking
A2.8 Certification of Standardized Test Block
X1. ADJUSTMENT OF KÖHLER ILLUMINATION SYSTEMS
X1.1
TABLE A2.1
TABLE A2.2
24 X2. CORRELATION OF MICROINDENTATION HARDNESS TEST DATA BETWEEN LABORATORIES
X2.1 Scope
X2.2 Correlation Procedure
X2.3 Referee
X3. RESULTS OF INTERLABORATORY TEST OF THE MEASUREMENT OF MICROINDENTATIONS
X3.1 Introduction
X3.2 Scope
X3.3 Procedure
X3.4 Results
25 TABLE X3.1
TABLE X3.2
TABLE X3.3
26 TABLE X3.4
FIG. X3.1
FIG. X3.2
27 FIG. X3.3
FIG. X3.4
28 X4. RESULTS OF AN INTERLABORATORY TEST COMPARING MICROINDENTATION HARDNESS TESTING USING MANUAL AND AUTOMATED MEASURING SYSTEMS
X4.1 Introduction
X4.2 Scope
X4.3 Procedure
X4.4 Repeatability
X4.5 Reproducibility
29 X4.6 Comparisons
TABLE X4.1
TABLE X4.2
TABLE X4.3
30 TABLE X4.4
FIG. X4.1
FIG. X4.2
31 FIG. X4.3
FIG. X4.4
32 FIG. X4.5
FIG. X4.6
33 X5. RECOMMENDATIONS FOR LIGHT FORCE MICROINDENTATION HARDNESS TESTING
X5.1 Introduction
FIG. X4.7
FIG. X4.8
34 X5.2 Scope
X5.3 Environment
X5.4 Specimens
X5.5 Instruments
35 X5.6 Measurement of Indentations
X5.7 Scanning Electron Microscope
X5.8 Video and Automatic Measuring Systems
X6. HK AND HV VALUES FOR A1 gf TEST LOAD
X6.1
TABLE X6.1
39 TABLE X6.2
43 REFERENCES
ASTM-E384 2011
$63.38