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BS ISO 16592:2012

$102.76

Microbeam analysis. Electron probe microanalysis. Guidelines for determining the carbon content of steels using a calibration curve method

Published By Publication Date Number of Pages
BSI 2012 22
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This International Standard gives guidance on a method for the determination of the carbon content in steels containing other alloying elements (less than 1 % to 2 % by mass) using the calibration curve method. It specifies the sample preparation, X-ray detection, establishment of the calibration curve and the procedure for the determination of the uncertainty of the measured carbon content. It is applicable to steels containing a mass fraction of carbon of less than 1,0 %. The method is not applicable to steels with higher carbon contents, which could significantly affect the accuracy of the analysis results.

This International Standard applies to analyses performed using normal beam incidence and wavelength-dispersive X-ray spectrometry; it is not designed to be used for energy-dispersive X-ray spectrometry.

PDF Catalog

PDF Pages PDF Title
3 CVP_Secretariat_Loca
6 Foreword
7 1 Scope
2 Procedure
2.1 General
2.2 Reference materials
2.3 Specimen preparation
8 2.4 Measurement of carbon Kα X‑ray intensity
9 2.5 Background subtraction
10 2.6 Establishment of the calibration curve
12 3 Evaluation of uncertainty
4 Test report
14 Annex A
(informative)

Method of estimating the uncertainty of the calculated value using a calibration curve

16 Annex B
(informative)

A practical example of the determination of the mass fraction of carbon and the evaluation of uncertainty in a steel

18 Bibliography
BS ISO 16592:2012
$102.76